{2,2′-[(1,2-Di­cyano­ethene-1,2-di­yl)bis­(nitrilo­methanylyl­idyne)]diphenolato-κ4 O,N,N′,O′}(methanol-κO)zinc

نویسندگان

  • Zhi-Chun Wang
  • Jing Chu
  • Shu-Zhong Zhan
چکیده

In the title complex, [Zn(C18H10N4O2)(CH4O)], the Zn(2+) cation is located on a mirror plane and is coordinated by a tetradentate Schiff base ligand anion (L (2-)) and a methanol mol-ecule. The Zn(2+) cation is surrounded by two N atoms and two O atoms from L (2-), in a nearly planar configuration, and one methanol O atom, forming a slightly distorted square-pyramidal geometry. The methanol molecule is disordered over two sets of sites in a 0.5:0.5 ratio. In the crystal, O-H⋯O hydrogen bonds link the mol-ecules into chains parallel to [001].

منابع مشابه

Chlorido[2,2′-[1,2-phenyl­enebis(nitrilo­methanylyl­idyne)]diphenolato-κ4 O,N,N′,O′]manganese(III) methanol monosolvate

In the title complex, [Mn(C20H14N2O2)Cl]·CH3OH, the central Mn(III) atom displays a distorted square-pyramidal coordination by two N and two O atoms from the tetradentate 2,2'-[1,2-phenyl-enebis(nitrilo-methanylyl-idyne)]diphenolate ligand and one chloride ligand. The Mn(III) atom is 0.525 (4) Å out of the square basal N2O2 least-squares plane. The complex mol-ecule is hydrogen bonded to the me...

متن کامل

{6,6′-Dimeth­oxy-2,2′-[(cyclo­hexane-1,2-di­yl)bis­(nitriliomethyl­idyne)]diphenolato}trinitratolanthanum(III) methanol monosolvate

In the title mononuclear complex, [La(NO(3))(3)(C(22)H(26)N(2)O(4))]·CH(3)OH, the La(III) ion is coordinated by three bidentate nitrate counter-ions and one zwitterionic 6,6'-dimeth-oxy-2,2'-[(cyclo-hexane-1,2- di-yl)bis-(nitriliomethyl-idyne)]diphenolate ligand through two phenolate and two meth-oxy O atoms, while the protonated N atoms remain uncoordinated. H atoms located on the two N atoms ...

متن کامل

The cocrystal aqua­chlorido{6,6′-di-tert-butyl-2,2′-[1,2-phenyl­enebis(nitrilo­methyl­idyne)]diphenolato-κ4 O,N,N′,O′}­manganese(III)–chlorido{6,6′-di-tert-butyl-2,2′-[1,2-phenyl­enebis(nitrilo­methyl­idyne)]diphenolato-κ4 O,N,N′,O′}(methanol-κO)manganese(III) (1/1)

The asymmetric unit of the title complex, [Mn(C(28)H(30)N(2)O(2))Cl(H(2)O)][Mn(C(28)H(30)N(2)O(2))Cl(CH(3)OH)], contains two discrete Mn(III) complexes of a Schiff base ligand, with an N(2)O(2) donor set. Both Mn(III) centers are in a distorted octa-hedral geometry with the N(2)O(2) donor atoms of the tetra-dentate Schiff base dianion in the equatorial plane. The axial positions in the coordina...

متن کامل

{4,4′,6,6′-Tetra­chloro-2,2′-[(spiro­[4.4]nonane-1,6-di­yl)bis­(nitrilo­methyl­idyne)]diphenolato-κ4 O,N,N′,O′}nickel(II)

The title compound, [Ni(C(23)H(20)Cl(4)N(2)O(2))], has an Ni(II) ion in a square-planar coordination formed by two imine N and two phenolato O atoms.

متن کامل

(Dimethyl sulfoxide-κO){4,4′,6,6′-tetra-tert-butyl-2,2′-[1,2-dicyano­ethene-1,2-diylbis(nitrilo­methyl­idyne)]diphenolato-κ4 O,N,N′,O′}zinc(II) acetonitrile monosolvate

The Zn atom in the title acetonitrile solvate, [Zn(C(34)H(42)N(4)O(2))(C(2)H(6)OS)]·CH(3)CN, exists in a distorted square-pyramidal geometry with the basal plane defined by the N(2)O(2) atoms of the tetra-dentate Schiff base and with the dimethyl sulfoxide O atom in the apical position. The tetra-dentate mode of coordination of the Schiff base ligand leads to a five-membered ZnN(2)C(2) chelate ...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

متن کامل
عنوان ژورنال:

دوره 69  شماره 

صفحات  -

تاریخ انتشار 2013